DOI:
铜业工程:2021(2):34-39
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高纯硝酸银制备工艺研究
(江西铜业集团有限公司 贵溪冶炼厂,江西 贵溪 335424)
Research Preparation Technology of High Purity Silver Nitrate
(Guixi Smelter, Jiangxi Copper Corporation Limited, Guixi 335424, Jiangxi, China)
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投稿时间:2020-12-28    
中文摘要: 以粗银粉为原料,采用硝酸浸出、氯化沉银、硝酸二次溶解、浓缩结晶、烘干等工序制备硝酸银产品。通过对硝酸银制备过程,浓度控制、温度控制、试剂添加量控制、除杂提纯等因素考察,开发了从粗银粉制备分析纯硝酸银的技术路线,成功制备出符合硝酸银国家标准(GB/T 670-2007)中分析纯硝酸银要求的成品。工艺取得较好的经济效益。
中文关键词: 硝酸银晶体  浓度  温度  除杂提纯  浓缩结晶
Abstract:With crude silver powder as raw material, silver nitrate products are prepared using nitric acid leaching, silver chloride,secondary dissolution of nitric acid, concentrated crystallization, drying and other processes. Through the silver nitrate preparation process, concentration control, temperature control, reagent addition control, de-hybrid purification and other factors, developed from the crude silver preparation analysis of pure silver nitrate technical route, successfully prepared in line with the national standard of silver nitrate (GB/T 670-2007) analysis of pure silver nitrate requirements of the finished product. The process has achieved better economic benefits.
文章编号:20210209     中图分类号:TF832
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引用文本: 孙敬韬,刘永平.高纯硝酸银制备工艺研究[J].铜业工程,2021,(2):34-39